The present paper deals with proper separation of trisodium phosphate as a valuable by product from the associated excess caustic soda of the reaction filtrate of controlled alkali breakdown of Rosetta monazite. Two procedures are applied for this purpose; namely a direct crystallization procedure of the phosphate product or else its salting out by using methanol.
XRD and IR analysis of the separated by-product indicated a structural formula of Na3PO4.12H2O. Analysis of the latter was revealed about 100 ppm uranium in the product separated by crystallization while that separated by methylation was completely exempt of uranium.
MAHMOUD, K., ABO-ALY, M., ALI, M., & EL-SHEIKH, A. (2006). RECOVERY OF NON-RADIOACTIVE TRI-SODIUM PHOSPHATE BY-PRODUCT THROUGH CONTROLLED ALKALI BREAKDOWN OF ROSETTA MONAZITE. Al-Azhar Bulletin of Science, 17(Issue 2-A), 43-52. doi: 10.21608/absb.2006.11652
MLA
KH. F. MAHMOUD; M. M. ABO-ALY; M. M. ALI; A. S. EL-SHEIKH. "RECOVERY OF NON-RADIOACTIVE TRI-SODIUM PHOSPHATE BY-PRODUCT THROUGH CONTROLLED ALKALI BREAKDOWN OF ROSETTA MONAZITE". Al-Azhar Bulletin of Science, 17, Issue 2-A, 2006, 43-52. doi: 10.21608/absb.2006.11652
HARVARD
MAHMOUD, K., ABO-ALY, M., ALI, M., EL-SHEIKH, A. (2006). 'RECOVERY OF NON-RADIOACTIVE TRI-SODIUM PHOSPHATE BY-PRODUCT THROUGH CONTROLLED ALKALI BREAKDOWN OF ROSETTA MONAZITE', Al-Azhar Bulletin of Science, 17(Issue 2-A), pp. 43-52. doi: 10.21608/absb.2006.11652
VANCOUVER
MAHMOUD, K., ABO-ALY, M., ALI, M., EL-SHEIKH, A. RECOVERY OF NON-RADIOACTIVE TRI-SODIUM PHOSPHATE BY-PRODUCT THROUGH CONTROLLED ALKALI BREAKDOWN OF ROSETTA MONAZITE. Al-Azhar Bulletin of Science, 2006; 17(Issue 2-A): 43-52. doi: 10.21608/absb.2006.11652
)
View on SCiNiTO